3U5S
Selenium Substituted Human Augmenter of Liver Regeneration
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2011-09-07 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54178 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.892, 76.878, 63.464 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.530 - 1.500 |
R-factor | 0.20731 |
Rwork | 0.205 |
R-free | 0.24353 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mbg |
RMSD bond length | 0.024 |
RMSD bond angle | 2.270 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.550 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.254 | |
Number of reflections | 15561 | |
<I/σ(I)> | 2.43 | |
Completeness [%] | 36.4 | |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | VAPOR DIFFUSION, HANGING DROP, temperature 298K |