3U2X
Crystal Structure of Human Glycogenin-1 (GYG1) complexed with manganese, UDP and 1'-deoxyglucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-11-22 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 46.700, 46.860, 69.700 |
Unit cell angles | 79.57, 88.96, 77.25 |
Refinement procedure
Resolution | 30.000 - 1.770 |
R-factor | 0.20002 |
Rwork | 0.198 |
R-free | 0.24661 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q4s |
RMSD bond length | 0.015 |
RMSD bond angle | 1.553 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.460 | 1.870 |
High resolution limit [Å] | 1.770 | 1.770 |
Rmerge | 0.075 | 0.538 |
Number of reflections | 50332 | |
<I/σ(I)> | 9.8 | 2.1 |
Completeness [%] | 91.1 | 87.6 |
Redundancy | 3.8 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293.15 | 1.4M tri-sodium citrate dihydrate, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |