3U08
Crystal structure of DB1963-D(CGCGAATTCGCG)2 complex at 1.25 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-08-07 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9796 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.070, 39.760, 65.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.330 - 1.250 |
R-factor | 0.20508 |
Rwork | 0.203 |
R-free | 0.24339 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.347 |
Data reduction software | xia2 |
Data scaling software | SCALA |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 24.070 | 1.380 | 1.180 |
High resolution limit [Å] | 1.150 | 1.330 | 1.150 |
Number of reflections | 32077 | ||
Completeness [%] | 74.2 | 79.4 | 8.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 283 | MAGNESIUM CHLORIDE, DNA, DB1963, MPD, SODIUM CACODYLATE BUFFER, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 283K |