Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

3TZR

Structure of a Riboswitch-like RNA-ligand complex from the Hepatitis C Virus Internal Ribosome Entry Site

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]173
Detector technologyIMAGE PLATE
Collection date2011-05-31
DetectorMAR scanner 345 mm plate
Wavelength(s)1.54
Spacegroup nameP 21 21 21
Unit cell lengths32.054, 33.582, 81.046
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution16.791 - 2.212
R-factor0.1815
Rwork0.179
R-free0.23800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2nok
RMSD bond length0.006
RMSD bond angle1.313
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]16.8002.280
High resolution limit [Å]2.2002.200
Number of reflections4664
Completeness [%]99.275.6
Redundancy6.74.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.528910 mM magnesium sulfate, 50 mM sodium cacodylate, 2.0 M ammonium sulfate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon