3TVD
Crystal Structure of Mouse RhoA-GTP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-03-21 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 80.813, 122.652, 91.276 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.999 - 2.989 |
R-factor | 0.2284 |
Rwork | 0.223 |
R-free | 0.28250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ftn |
RMSD bond length | 0.009 |
RMSD bond angle | 1.130 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.000 | 3.150 |
High resolution limit [Å] | 2.989 | 3.000 |
Number of reflections | 8595 | |
Completeness [%] | 99.7 | 99 |
Redundancy | 4.9 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 0.2M Ammonium acetate, 0.1M Sodium acetate (pH4.6), 30% Polyethylene glycol 4000, VAPOR DIFFUSION, HANGING DROP, temperature 298K |