3TTL
Crystal structure of apo-SpuE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-09-18 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.323, 48.841, 114.334 |
Unit cell angles | 90.00, 103.24, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.2207 |
Rwork | 0.218 |
R-free | 0.26997 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ttn |
RMSD bond length | 0.011 |
RMSD bond angle | 1.381 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.510 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 30162 | |
Completeness [%] | 96.8 | 79.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 288 | 0.1M Tris, 0.2M MgCl2, 25% PEG 3350, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 288K |