3TT6
Structure of ClpP from Bacillus subtilis in compressed state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-26 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 109.090, 172.864, 83.427 |
Unit cell angles | 90.00, 118.93, 90.00 |
Refinement procedure
Resolution | 36.088 - 2.592 |
R-factor | 0.2238 |
Rwork | 0.221 |
R-free | 0.27680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ce3 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.354 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7_650) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.690 |
High resolution limit [Å] | 2.592 | 5.600 | 2.600 |
Rmerge | 0.072 | 0.049 | 0.503 |
Number of reflections | 41517 | ||
<I/σ(I)> | 13.6 | ||
Completeness [%] | 99.4 | 99.3 | 94.6 |
Redundancy | 3.6 | 3.6 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | 5.6 | 295 | 0.1M sodium citrate, 0.1M lithium sulfate, 10-12%(w/v) PEG 4000, pH 5.6, hanging drop, temperature 295K |