3TMV
X-Ray Radiation Damage to HEWL Crystals soaked in 100mM Sodium Nitrate (Dose=0.12MGy)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 295 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.241 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 79.876, 79.876, 38.736 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.720 - 1.900 |
| R-factor | 0.15514 |
| Rwork | 0.152 |
| R-free | 0.21913 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.027 |
| RMSD bond angle | 1.969 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | BUSTER |
| Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 56.480 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 10377 |
| Completeness [%] | 100.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
