3TMM
TFAM imposes a U-turn on mitochondrial DNA
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-18 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97864, 0.91837, 0.97898 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 68.438, 81.911, 161.254 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.192 - 2.500 |
R-factor | 0.1973 |
Rwork | 0.195 |
R-free | 0.24780 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.225 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.6_289)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 24.192 | 25.000 | 2.640 |
High resolution limit [Å] | 2.500 | 7.910 | 2.500 |
Rmerge | 0.074 | ||
Number of reflections | 15812 | ||
<I/σ(I)> | 10.6 | ||
Completeness [%] | 99.8 | 87.9 | 99.5 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 298 | 29% PEG 400, 0.15 M calcium acetate, 0.1 M sodium acetate,pH 4.2, 400 mM NDSB211, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 298 | 29% PEG 400, 0.15 M calcium acetate, 0.1 M sodium acetate,pH 4.2, 400 mM NDSB211, VAPOR DIFFUSION, HANGING DROP, temperature 298K |