3TJN
HtrA1 catalytic domain, apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2008-10-07 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 108.495, 108.495, 234.435 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 3.000 |
R-factor | 0.24449 |
Rwork | 0.242 |
R-free | 0.29372 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lcy |
RMSD bond length | 0.008 |
RMSD bond angle | 1.171 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.000 |
Number of reflections | 16292 |
<I/σ(I)> | 27 |
Completeness [%] | 95.0 |
Redundancy | 11 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 300 | ammonium acetate, pH 7, VAPOR DIFFUSION, SITTING DROP, temperature 300K |