3TEC

CALCIUM BINDING TO THERMITASE. CRYSTALLOGRAPHIC STUDIES OF THERMITASE AT 0, 5 AND 100 MM CALCIUM

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	65.240, 71.770, 88.990
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.000
R-factor	0.168 *
Rwork	0.168
RMSD bond length	0.018
RMSD bond angle	2.700
Refinement software	GROMOS

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.066 *
Total number of observations	91303 *
Number of reflections	22550 *
Completeness [%]	78.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Thermitase-eglin-c crystals
2	1	drop		100 (mM)
3	1	reservoir	Bis-Tris	50 (mM)
4	1	reservoir	PEG6000	25 (%)
5	1	resrvoir		100 (mM)