3T9L
Structure of N-terminal DUSP-UBL domains of human USP15
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9763 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 97.601, 97.601, 69.398 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.262 - 1.500 |
R-factor | 0.1585 |
Rwork | 0.156 |
R-free | 0.17780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 1W6V and 3JYU |
RMSD bond length | 0.005 |
RMSD bond angle | 0.934 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.16) |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 84.525 | 84.525 | 1.560 |
High resolution limit [Å] | 1.479 | 4.680 | 1.480 |
Rmerge | 0.068 | 0.292 | |
Total number of observations | 36566 | 82766 | |
Number of reflections | 63890 | ||
<I/σ(I)> | 22.5 | 8.5 | 2.6 |
Completeness [%] | 99.7 | 100 | 97.9 |
Redundancy | 10.5 | 16.8 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 298 | 2M ammonium sulphate, 100 mM Bis-Tris-Cl, pH 5.5, vapor diffusion, temperature 298K |