3T7O
Crystal Structure of Human Glycogenin-1 (GYG1) complexed with manganese, UDP-Glucose and glucose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-12-20 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 46.415, 46.590, 69.904 |
Unit cell angles | 79.54, 88.75, 75.83 |
Refinement procedure
Resolution | 28.330 - 1.850 |
R-factor | 0.19809 |
Rwork | 0.195 |
R-free | 0.25501 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3q4s |
RMSD bond length | 0.015 |
RMSD bond angle | 1.620 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.400 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.094 | 0.424 |
Number of reflections | 44222 | |
<I/σ(I)> | 9.5 | 2.8 |
Completeness [%] | 92.9 | 88.5 |
Redundancy | 3.8 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293.15 | 2.0M Ammonium Sulphate, 0.1M Bis-Tris, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |