3T3X
1.57 A structure of Friedreich's ataxia frataxin variant R165C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Detector technology | CCD |
Detector | NOIR-1 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 86.020, 32.120, 92.080 |
Unit cell angles | 90.00, 90.16, 90.00 |
Refinement procedure
Resolution | 19.500 - 1.570 |
R-factor | 0.21821 |
Rwork | 0.216 |
R-free | 0.25124 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.025 |
RMSD bond angle | 2.357 |
Data reduction software | XFIT |
Data scaling software | SCALA |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.500 | 1.611 |
High resolution limit [Å] | 1.570 | 1.570 |
Number of reflections | 35106 | |
Completeness [%] | 98.8 | 97.45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 295 | 1.9 M ammonium sulfate, 0.1 M sodium citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |