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3T3T

1.38 A structure of human frataxin variant Q148G

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL11-1
Synchrotron siteSSRL
BeamlineBL11-1
Detector technologyCCD
DetectorMARMOSAIC 325 mm CCD
Wavelength(s)1.0971
Spacegroup nameP 1 21 1
Unit cell lengths46.410, 68.560, 89.970
Unit cell angles90.00, 93.23, 90.00
Refinement procedure
Resolution26.190 - 1.380
R-factor0.19947
Rwork0.198
R-free0.22656
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.032
RMSD bond angle2.500
Data reduction softwareXFIT
Data scaling softwareSCALA
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.1901.416
High resolution limit [Å]1.3801.380
Number of reflections111516
Completeness [%]96.794.24
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.52952.0 M ammonium sulfate, 0.1 M citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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PDB entries from 2024-11-06

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