3T1S
MglB Homodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-07-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9300 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 36.150, 36.150, 308.770 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.300 - 1.670 |
R-factor | 0.2212 |
Rwork | 0.219 |
R-free | 0.27229 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1j3w |
RMSD bond length | 0.023 |
RMSD bond angle | 2.118 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.300 | 1.710 |
High resolution limit [Å] | 1.670 | 1.670 |
Number of reflections | 15213 | |
Completeness [%] | 99.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293.15 | 0.28M CaCl2, 7% Isopropanol, 30% Glycerol, 0.07 M Natrium-Acetate , pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293.15K |