3T1K
HSP90 N-terminal domain bound to ANP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 1 |
| Unit cell lengths | 43.274, 55.969, 60.535 |
| Unit cell angles | 93.39, 95.82, 112.49 |
Refinement procedure
| Resolution | 29.940 - 1.500 |
| R-factor | 0.1626 |
| Rwork | 0.162 |
| R-free | 0.18880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1yes |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.572 |
| Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.500 |
| Rmerge | 0.068 |
| Number of reflections | 79738 |
| <I/σ(I)> | 18.994 |
| Completeness [%] | 96.0 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
