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3SZ5

Crystal Structure of LHK-Exo in complex with 5-phosphorylated oligothymidine (dT)4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2010-01-02
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameP 63
Unit cell lengths108.697, 108.697, 48.219
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.000 - 2.800
R-factor0.1958
Rwork0.193
R-free0.24772
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3syy
RMSD bond length0.014
RMSD bond angle1.550
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0044)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.850
High resolution limit [Å]2.8002.800
Rmerge0.0670.492
Number of reflections8198
<I/σ(I)>35.53.4
Completeness [%]99.9100
Redundancy6.86.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.42930.1M Tris pH 8.4, 1.0M potassium sodium tartrate tetrahydrate, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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