3SYB
Crystal structure of Pseudomonas aeruginosa OccD3 (OpdP)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-17 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.972 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 99.930, 159.828, 82.064 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.993 - 2.700 |
R-factor | 0.2194 |
Rwork | 0.214 |
R-free | 0.26710 |
Structure solution method | P |
RMSD bond length | 0.008 |
RMSD bond angle | 1.163 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.710 |
High resolution limit [Å] | 2.660 | 2.660 |
Number of reflections | 18213 | |
Completeness [%] | 92.9 | 96.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 295 | 25% PEG 1000 0.2 M ammonium sulphate 50 mM Na-citrate, pH 4.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |