3SY9
Crystal structure of Pseudomonas aeruginosa OccD2 (OpdC)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-17 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97 |
Spacegroup name | P 1 |
Unit cell lengths | 93.353, 102.828, 101.696 |
Unit cell angles | 77.67, 62.57, 62.95 |
Refinement procedure
Resolution | 14.957 - 2.800 |
R-factor | 0.2179 |
Rwork | 0.216 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.296 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.840 |
High resolution limit [Å] | 2.790 | 2.790 |
Number of reflections | 105852 | |
Completeness [%] | 83.2 | 73.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 295 | 25% PEG 4000 15 mM Tricine, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |