3SWM
The NAC domain of ANAC019 in complex with DNA, gold derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-09-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.038 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.530, 109.070, 173.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.203 - 4.250 |
R-factor | 0.2562 |
Rwork | 0.250 |
R-free | 0.30920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1UT7 + B-DNA model |
RMSD bond length | 0.015 |
RMSD bond angle | 2.285 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.203 | 4.450 |
High resolution limit [Å] | 4.250 | 4.250 |
Number of reflections | 9600 | |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.01 M magnesium sulfate, 0.05 M MES, pH 6.5, 0.5% PEG400, VAPOR DIFFUSION, HANGING DROP, temperature 298K |