Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-D |
| Synchrotron site | APS |
| Beamline | 23-ID-D |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-06-28 |
| Detector | MARMOSAIC 300 mm CCD |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 95.889, 95.889, 795.391 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 49.270 - 2.150 |
| R-factor | 0.262 |
| Rwork | 0.261 |
| R-free | 0.29100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | PDB entries 3GQ7 3gqh |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.088 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.270 | 2.230 |
| High resolution limit [Å] | 2.150 | 2.150 |
| Rmerge | 0.146 | 0.446 |
| Number of reflections | 68349 | |
| <I/σ(I)> | 17.143 | |
| Completeness [%] | 88.0 | 57 |
| Redundancy | 15.6 | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 3.0 M Sodium Acetate at pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
