Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-27 |
| Detector | BRUKER SMART 6000 |
| Wavelength(s) | 1.54188 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 66.560, 66.560, 136.720 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 59.870 - 2.140 |
| R-factor | 0.21831 |
| Rwork | 0.216 |
| R-free | 0.25361 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2aai |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.980 |
| Data reduction software | SAINT |
| Data scaling software | SADABS |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 68.360 | 2.230 |
| High resolution limit [Å] | 2.140 | 2.140 |
| Number of reflections | 17463 | |
| <I/σ(I)> | 21.11 | 4.39 |
| Completeness [%] | 98.5 | 87.4 |
| Redundancy | 12.35 | 6.13 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 290 | 30% Ammonium Sulfate, 50 mM Sodium Acetate pH 4.2, VAPOR DIFFUSION, HANGING DROP, temperature 290K |
