Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Detector technology | CCD |
Collection date | 2010-01-01 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 133.046, 73.236, 138.023 |
Unit cell angles | 90.00, 96.80, 90.00 |
Refinement procedure
Resolution | 22.100 - 2.100 |
R-factor | 0.2272 |
Rwork | 0.225 |
R-free | 0.27190 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.509 |
Data scaling software | SCALA |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 22.100 |
High resolution limit [Å] | 2.100 |
Number of reflections | 147820 |
Completeness [%] | 95.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Sitting Batch | 7.2 | 298 | PEG 8000, pH 7.2, Sitting Batch, temperature 298K |