3SQI
DNA binding domain of Ndc10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2009-06-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97914 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 117.303, 147.536, 95.639 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.388 - 2.825 |
R-factor | 0.1962 |
Rwork | 0.193 |
R-free | 0.25110 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 1.147 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.113 | 0.717 |
Number of reflections | 18620 | |
<I/σ(I)> | 23.8 | 2 |
Completeness [%] | 91.3 | 74.2 |
Redundancy | 14.7 | 11.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 20% PEG400, 0.1 M MES pH 6.0, 0.2 M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 298K |