3SOK
Dichelobacter nodosus pilin FimA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 105.729, 105.729, 73.848 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.283 - 2.300 |
R-factor | 0.2393 |
Rwork | 0.234 |
R-free | 0.29020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB code 2HI2 conserved core (residues 1-55 + 78-92 + 105-111) |
RMSD bond length | 0.008 |
RMSD bond angle | 1.098 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.300 | 2.520 |
High resolution limit [Å] | 2.000 | 2.300 |
Number of reflections | 27380 | |
Completeness [%] | 96.5 | 97.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 295 | 60% saturated ammonium sulfate 5% saturated NaCl 100mM Na Citrate 5% 1M NaPO4, pH 9.23, VAPOR DIFFUSION, HANGING DROP, temperature 295K |