3SK7
Crystal Structure of V. cholerae SeqA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-30 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 29.008, 55.029, 135.534 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.918 - 1.500 |
R-factor | 0.1587 |
Rwork | 0.156 |
R-free | 0.20360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fmt |
RMSD bond length | 0.010 |
RMSD bond angle | 1.068 |
Refinement software | PHENIX ((phenix.refine: 1.7_650)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.490 |
High resolution limit [Å] | 1.460 | 1.460 |
Rmerge | 0.082 | 0.462 |
Number of reflections | 35671 | |
<I/σ(I)> | 21.266 | 4.403 |
Completeness [%] | 99.6 | 98.3 |
Redundancy | 6.9 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 30% PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 277K | |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 30% PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 277K |