Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 291 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.490, 91.000, 66.160 |
Unit cell angles | 90.00, 104.36, 90.00 |
Refinement procedure
Resolution | 40.060 - 2.500 |
R-factor | 0.1857 |
Rwork | 0.183 |
R-free | 0.24425 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.360 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASES |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.100 |
High resolution limit [Å] | 1.900 |
Number of reflections | 39194 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | PEG4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |