3SGB

STRUCTURE OF THE COMPLEX OF STREPTOMYCES GRISEUS PROTEASE B AND THE THIRD DOMAIN OF THE TURKEY OVOMUCOID INHIBITOR AT 1.8 ANGSTROMS RESOLUTION

Replaces:  2SGBReplaces:  1SGB

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	45.350, 54.520, 45.650
Unit cell angles	90.00, 119.20, 90.00

Refinement procedure

Resolution	6.000 - 1.800
R-factor	0.125 *
Rwork	0.125
RMSD bond length	0.017 *
RMSD bond angle	0.037 *

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	2.000 *
Total number of observations	13937 *
Number of reflections	18082 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop		10 (mM)
2	1	drop	enzyme	10-15 (mg/ml)
3	1	reservoir		1.0 (M)	precipitant
4	1	reservoir		0.7-1.0 (M)	precipitant