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3SG8

Crystal Structure of Aminoglycoside-2''-Phosphotransferase Type IVa Tobramycin Complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCLSI BEAMLINE 08ID-1
Synchrotron siteCLSI
Beamline08ID-1
Temperature [K]93
Detector technologyCCD
Collection date2011-02-25
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.9795
Spacegroup nameP 1 21 1
Unit cell lengths43.334, 101.479, 73.455
Unit cell angles90.00, 100.78, 90.00
Refinement procedure
Resolution33.990 - 1.800
R-factor0.18828
Rwork0.185
R-free0.24208
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.023
RMSD bond angle1.889
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.860
High resolution limit [Å]1.5601.800
Number of reflections57440
<I/σ(I)>4.1
Completeness [%]99.498.9
Redundancy5.15.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.527750 mM HEPES, 17% PEG4000, 10% glycerol, 5% isopropanol, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 277K

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