3SAV
MUTM Slanted complex 8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.455, 94.240, 104.218 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.665 - 2.125 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.21850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2f5o |
RMSD bond length | 0.007 |
RMSD bond angle | 1.034 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.210 |
High resolution limit [Å] | 2.125 | 2.125 |
Rmerge | 0.088 | 0.492 |
Number of reflections | 25440 | |
<I/σ(I)> | 10.5 | |
Completeness [%] | 97.8 | 93.8 |
Redundancy | 5.4 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 298 | PEG 8K, SODIUM CACODYLATE, GLYCEROL, PH 7.0, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 298K |