3SAU
MUTM Interrogation complex 6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.423, 93.436, 104.920 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.250 - 1.650 |
R-factor | 0.189 |
Rwork | 0.188 |
R-free | 0.21300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gpx |
RMSD bond length | 0.006 |
RMSD bond angle | 1.086 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.057 | 0.493 |
Number of reflections | 52738 | |
<I/σ(I)> | 13.4 | |
Completeness [%] | 96.6 | 92.2 |
Redundancy | 5.5 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 291 | PEG 8K, SODIUM CACODYLATE, GLYCEROL, PH 7.0, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 291K |