3S7V
Unassembled KI Polyomavirus VP1 Pentamer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-02-24 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 70.330, 82.780, 142.060 |
Unit cell angles | 87.01, 98.23, 108.65 |
Refinement procedure
Resolution | 49.270 - 2.550 |
R-factor | 0.20332 |
Rwork | 0.202 |
R-free | 0.21939 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.252 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.620 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.054 | 0.602 |
Number of reflections | 93982 | |
<I/σ(I)> | 11.9 | 1.4 |
Completeness [%] | 95.9 | 91.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 0.2 M sodium formate pH 7.0, 20 % (w/v) PEG 3350, VAPOR DIFFUSION, SITTING DROP, temperature 298K |