3S6W
Crystal structure of Tudor domain of human TDRD3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-08-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 65 |
Unit cell lengths | 41.930, 41.930, 61.478 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.310 - 1.780 |
R-factor | 0.18397 |
Rwork | 0.183 |
R-free | 0.20618 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mhn |
RMSD bond length | 0.011 |
RMSD bond angle | 1.138 |
Data reduction software | DENZO |
Data scaling software | d*TREK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 36.310 | 1.920 | 1.840 |
High resolution limit [Å] | 1.780 | 1.840 | 1.780 |
Number of reflections | 5836 | ||
Completeness [%] | 98.4 | 99.8 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 290 | 10% 2-propanol, 100mM Phosphate-Citrate, 0.2M Li2SO4, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K |