3S2Q

The crystal structure of AT5g51720 (AT-NEET)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Collection date	2010-11-15
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.92
Spacegroup name	P 21 21 21
Unit cell lengths	41.548, 60.090, 66.383
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.550 - 1.750
R-factor	0.183
Rwork	0.181
R-free	0.22700
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3ew0
RMSD bond length	0.014
RMSD bond angle	1.855
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall
Low resolution limit [Å]	44.550
High resolution limit [Å]	1.750
Number of reflections	16531
Completeness [%]	94.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	277	100mM ZnAc2 and 20% PEG 3350, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K