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3S0F

Apis mellifera OBP14 native apo, crystal form 2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsCu FINE FOCUS
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2011-03-11
DetectorMAR scanner 345 mm plate
Spacegroup nameP 21 21 2
Unit cell lengths64.080, 75.380, 42.140
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution37.690 - 2.030
R-factor0.1956
Rwork0.194
R-free0.21840
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3s0a
RMSD bond length0.010
RMSD bond angle1.240
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareMOLREP
Refinement softwareBUSTER (2.9.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]45.2002.080
High resolution limit [Å]2.0302.030
Rmerge0.0290.080
Number of reflections13308
<I/σ(I)>26.412
Completeness [%]96.573.6
Redundancy2.82.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP629330% PEG4000, 10 mM imidazole-malate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K

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