3RYI
GDP-Tubulin: rb3 stathmin-like domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-13 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.720, 127.600, 250.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.590 - 2.400 |
R-factor | 0.1686 |
Rwork | 0.167 |
R-free | 0.20090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hkb |
RMSD bond length | 0.009 |
RMSD bond angle | 1.160 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AMoRE |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.590 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 81775 | |
<I/σ(I)> | 16.2 | 2.1 |
Completeness [%] | 97.5 | 81 |
Redundancy | 8.8 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.8 | 293 | PEG, LISO4, PIPES BUFFER, pH 6.80, VAPOR DIFFUSION, HANGING DROP, temperature 293K |