Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ELLIOTT GX-20 |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1991-06-11 |
| Detector | San Diego Multiwire Systems |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 72.740, 78.490, 114.340 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.910 - 3.000 |
| Rwork | 0.198 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.014 |
| RMSD bond angle | 4.000 |
| Data reduction software | San (Diego Multiwire Systems) |
| Data scaling software | San (Diego Multiwire Systems) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 3.000 |
| Number of reflections | 8250 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | batch | 4.75 | 298 | 11.5% PEG 8000, 0.05 M sodium acetate, 2 mM lactose, pH 4.75, batch, temperature 298K |
