3RQR
Crystal structure of the RYR domain of the rabbit ryanodine receptor
Experimental procedure
Experimental method | SAD |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-04-10 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 68.770, 68.770, 91.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.930 - 2.160 |
R-factor | 0.238 |
Rwork | 0.231 |
R-free | 0.25800 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.030 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | SHELXS |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.200 |
High resolution limit [Å] | 2.160 | 2.160 |
Rmerge | 0.103 | 0.846 |
Number of reflections | 12353 | |
<I/σ(I)> | 19.7 | 2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.2 | 8.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 291 | 1.2M Na Citrate, 100mM Tris pH8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K | |
1 | 8.5 | 291 | 1.2M Na Citrate, 100mM Tris pH8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |