Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | OTHER |
Temperature [K] | 277 |
Detector technology | FILM |
Collection date | 1989-11-01 |
Detector | CEA Reflex 25 |
Wavelength(s) | 1.10 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 86.200, 86.200, 35.660 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.400 - 1.650 |
R-factor | 0.17574 |
Rwork | 0.175 |
R-free | 0.19848 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 2MM1 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.995 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.400 |
High resolution limit [Å] | 1.650 |
Rmerge | 0.080 |
Number of reflections | 17640 |
Completeness [%] | 95.0 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 250 mM Tris-HCl, 80% Ammonium Sulfate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |