3RFY
Crystal structure of arabidopsis thaliana cyclophilin 38 (ATCYP38)
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 103 |
| Detector technology | CCD |
| Collection date | 2006-06-09 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9797, 0.9794, 0.9500 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 57.690, 96.720, 166.820 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.890 - 2.390 |
| R-factor | 0.248 |
| Rwork | 0.248 |
| R-free | 0.26600 |
| Structure solution method | MAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 2.900 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SnB |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.550 |
| High resolution limit [Å] | 2.390 | 2.450 |
| Number of reflections | 19441 | |
| <I/σ(I)> | 19.21 | 5.1 |
| Completeness [%] | 98.6 | 91.6 |
| Redundancy | 6.4 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 5.5 | 293 | 20% PEG 6000, 2.5% T-BUTANOL, 100MM SODIUM CITRATE (PH 5.5), VAPOR BATCH, TEMPERATURE 293K, VAPOR DIFFUSION |
