3RFF
Phosphopantetheine adenylyltransferase from Mycobacterium Tuberculosis (1.76 A resolution)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.8 |
Spacegroup name | H 3 2 |
Unit cell lengths | 98.678, 98.678, 113.855 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.995 - 1.760 |
R-factor | 0.1772 |
Rwork | 0.175 |
R-free | 0.22430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tfu |
RMSD bond length | 0.006 |
RMSD bond angle | 0.889 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 1.600 |
Rmerge | 0.044 |
Number of reflections | 28293 |
Completeness [%] | 91.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |