3RDV
Structure of the SLAIN2c-CLIPCG1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-10 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 1 |
Unit cell lengths | 38.210, 45.740, 49.360 |
Unit cell angles | 100.06, 105.76, 108.39 |
Refinement procedure
Resolution | 45.536 - 1.750 |
R-factor | 0.1836 |
Rwork | 0.180 |
R-free | 0.22880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2e3i |
RMSD bond length | 0.009 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | BALBES |
Refinement software | PHENIX (dev_279) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.540 | 1.800 | |
High resolution limit [Å] | 1.750 | 10.000 | 1.750 |
Rmerge | 0.069 | 0.036 | 0.349 |
Rmeas | 0.040 | 0.382 | |
Number of reflections | 28615 | 155 | 2254 |
<I/σ(I)> | 17.56 | 35.95 | 4.91 |
Completeness [%] | 96.8 | 98.7 | 95.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.5 | 298 | 36% PEG 6000, 100mM citric acid, pH 4.5, vapor diffusion, temperature 298K |