3RDJ
Rat PKC C2 domain Apo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 150 |
Detector technology | IMAGE PLATE |
Collection date | 2010-11-24 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.542 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 58.000, 58.000, 90.460 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.110 - 1.900 |
R-factor | 0.225 |
Rwork | 0.225 |
R-free | 0.24500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.670 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 14022 | |
Completeness [%] | 99.8 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 20% PEG3350, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |