3RC3
Human Mitochondrial Helicase Suv3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-14 |
Detector | MARMOSAIC 300 mm CCD |
Spacegroup name | P 32 |
Unit cell lengths | 89.390, 89.390, 88.070 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.840 - 2.080 |
R-factor | 0.161 |
Rwork | 0.160 |
R-free | 0.20300 |
Structure solution method | SAD |
RMSD bond length | 0.026 |
RMSD bond angle | 2.021 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SHELXD |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.150 |
High resolution limit [Å] | 2.080 | 2.080 |
Rmerge | 0.057 | 0.326 |
Number of reflections | 47146 | |
<I/σ(I)> | 15 | 3.49 |
Completeness [%] | 99.6 | 96.5 |
Redundancy | 3.8 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 277 | 6% PEG 3350, 0.1 M Na citrate, 10 % glycerol, pH 6.5, vapor diffusion, hanging drop, temperature 277K |