3RB7
Crystal structure of CBD12 from CALX1.2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-24 |
Detector | NOIR-1 |
Wavelength(s) | 1.000 |
Spacegroup name | H 3 |
Unit cell lengths | 107.535, 107.535, 358.650 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 119.500 - 2.900 |
Rwork | 0.231 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.255 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 119.500 |
High resolution limit [Å] | 2.900 |
Number of reflections | 34280 |
Completeness [%] | 91.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 5.5 | 291 | 0.1 M Bis-Tris, 0.4 M ammonium sulfate, 16% Polyethylene glycol 3350, pH 5.5, EVAPORATION, temperature 291K |