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3RAT

EFFECTS OF TEMPERATURE ON PROTEIN STRUCTURE AND DYNAMICS: X-RAY CRYSTALLOGRAPHIC STUDIES OF THE PROTEIN RIBONUCLEASE-A AT NINE DIFFERENT TEMPERATURES FROM 98 TO 320 K

Experimental procedure
Spacegroup nameP 1 21 1
Unit cell lengths29.510, 38.080, 52.930
Unit cell angles90.00, 106.32, 90.00
Refinement procedure
Resolution? - 1.500
R-factor0.149
RMSD bond length0.019
RMSD bond angle0.033
Refinement softwarePROLSQ
Data quality characteristics
 Overall
High resolution limit [Å]1.500

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RmergeNaN

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Number of reflections15873

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Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein12 (mg/ml)
2110.2 (M)
311methanol50 (%(v/v))

229183

PDB entries from 2024-12-18

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