3RA6
Crystal structure of T. celer L30e E62A/K46A variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2009-01-15 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 23.587, 53.913, 34.298 |
Unit cell angles | 90.00, 109.16, 90.00 |
Refinement procedure
Resolution | 32.398 - 2.000 |
R-factor | 0.2016 |
Rwork | 0.196 |
R-free | 0.25320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1h7m |
RMSD bond length | 0.007 |
RMSD bond angle | 1.008 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.398 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.077 | 0.174 |
Number of reflections | 5520 | |
<I/σ(I)> | 15.2 | 4.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 2.8 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 289 | 5% PEG MME 2000, 0.1M MES, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 289K |