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3R69

Molecular analysis of the interaction of the HDL-receptor SR-BI with the PDZ3 domain of its adaptor protein PDZK1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X12C
Synchrotron siteNSLS
BeamlineX12C
Temperature [K]100
Detector technologyCCD
Collection date2010-04-10
DetectorADSC QUANTUM 210
Wavelength(s)0.978
Spacegroup nameP 21 21 21
Unit cell lengths47.638, 61.396, 64.010
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution23.930 - 1.499
R-factor0.2016
Rwork0.200
R-free0.22549
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3r68
RMSD bond length0.018
RMSD bond angle1.718
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.5.0109)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.550
High resolution limit [Å]1.4991.499
Number of reflections29138
Completeness [%]94.566.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP3.52910.1 M citric acid pH 3.5, 25% PEG 3350, 5% ethylene glycol, VAPOR DIFFUSION, SITTING DROP, temperature 291K

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