3R3M
Crystal structure of the FAF1 UBX domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-03-06 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 61 |
Unit cell lengths | 92.755, 92.755, 108.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.645 - 3.000 |
R-factor | 0.1782 |
Rwork | 0.174 |
R-free | 0.25780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3qq8 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.324 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.6.2_432) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.340 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.095 | 0.518 |
Number of reflections | 10693 | |
<I/σ(I)> | 12.5 | 2.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.2 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | 0.4 M NaH2PO4/1.6 M K2HPO4, 0.1 M imidazole, 0.2 M NaCl, pH 8, VAPOR DIFFUSION, SITTING DROP, temperature 298K |